CAS 1263166-90-0 | BCN-OH
Molecular Formula: C10H14O
Molecular Weight: 150.22
Purity: 97% Min.
Package: 1 g / 5 g / 25 g / 100 g / 1 kg
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Product Introduction
Specification of CAS 1263166-90-0 | BCN-OH
ITEMS | SPECIFICATION |
Melting point | 64 °C |
Storage temp. | -20°C |
Density | 1.08 g/cm3 |
Boiling point | 256.5 °C |
pka | 14.95 |
BRN | 21037713 |
Synthesis of CAS 1263166-90-0 | BCN-OH
Conditions
Stage #1: C12H18O2 With diisobutylaluminium hydride In diethyl ether at 0 - 20℃;
Stage #2: With bromine In dichloromethane at 20℃; for 0.0833333h;
Stage #3: With potassium tert-butylate In tetrahydrofuran at 0℃; for 1.5h; Reflux;
Reference
Baalmann, Mathis; Bitsch, Sebastian; Deweid, Lukas; Ilkenhans, Nadja; Kolmar, Harald; Neises, Laura; Schneider, Hendrik; (…) Wombacher, Richard; Ziegler, Michael J.
[Angewandte Chemie - International Edition, 2020, vol. 59, # 31, p. 12885 - 12893]
[Angew. Chem., 2020, vol. 132, # 31, p. 12985 - 12993,9]
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