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CAS 894086-00-1 | 5-(DI-TERT-BUTYLPHOSPHINO)-1', 3', 5'-TRIPHENYL-1'H-[1,4']BIPYRAZOLE
Molecular Formula: C32H35N4P
Molecular Weight: 506.62
Purity: 97% Min.
Package: 1 g / 5 g / 25 g / 100 g / 1 kg
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Product Introduction
Specification of CAS 894086-00-1 | 5-(DI-TERT-BUTYLPHOSPHINO)-1', 3', 5'-TRIPHENYL-1'H-[1,4']BIPYRAZOLE
ITEMS | SPECIFICATION |
Melting point | 169-173 °C |
InChIKey | PTXJGGGNGMPMBG-UHFFFAOYSA-N |
Storage temp. | Inert atmosphere,Room Temperature |
Color | White to tan |
Form | Solid |
Water Solubility | Slightly soluble in water. |
Boiling point | 652.7 °C |
pka | -0.35 |
Sensitive | Air Sensitive |
Synthesis of CAS 894086-00-1 | 5-(DI-TERT-BUTYLPHOSPHINO)-1', 3', 5'-TRIPHENYL-1'H-[1,4']BIPYRAZOLE
Conditions
With n-butyllithium In tetrahydrofuran at -78 - 20℃; for 3.5h;
Reference
Singer, Robert A.; Doré, Michaël; Sieser, Janice E.; Berliner, Martin A.
[Tetrahedron Letters, 2006, vol. 47, # 22, p. 3727 - 3731]
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