CAS 97165-77-0 | 3,5-DIBROMOBENZONITRILE

Specification of CAS 97165-77-0 | 3,5-DIBROMOBENZONITRILE

Synthesis of CAS 97165-77-0 | 3,5-DIBROMOBENZONITRILE

Conditions

Stage #1: 1,3,5-trisbromobenzene With isopropylmagnesium chloride; lithium chloride In tetrahydrofuran at -15℃; for 0.25h;

Stage #2: With N,N-dimethyl-formamide In tetrahydrofuran at 0℃; for 2h; Stage #3: With ammonia; iodine In tetrahydrofuran; water at 20℃; for 2h;

Reference

Ishii, Genki; Harigae, Ryo; Moriyama, Katsuhiko; Togo, Hideo

[Tetrahedron, 2013, vol. 69, # 5, p. 1462 - 1469]

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