CAS 90259-31-7 | 2-Bromo-6-methylbenzoic Acid
Molecular Formula: C8H7BrO2
Molecular Weight: 215.04
Purity: 97% Min.
Package: 1 g / 5 g / 25 g / 100 g / 1 kg / 25 kg
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Product Introduction
Specification of CAS 90259-31-7 | 2-Bromo-6-methylbenzoic acid
ITEMS | SPECIFICATION |
Melting point | 108-112 °C |
storage temp. | Sealed in dry,Room Temperature |
density | 1.599 g/cm3 |
Boiling point | 307.0 °C |
pka | 2.56 |
BRN | 2614094 |
CAS DataBase Reference | 90259-31-7(CAS DataBase Reference) |
Synthesis of CAS 90259-31-7 | 2-Bromo-6-methylbenzoic acid
Conditions
Stage #1: 2-amino-6-methylbenzoic acid With hydrogen bromide; acetic acid; sodium nitrite In water at 0℃; Sandmeyer Reaction; Inert atmosphere;
Stage #2: With copper(I) bromide In water at 0 - 65℃; Sandmeyer Reaction; Inert atmosphere;
Reference
Chu, John C. K.; Dalton, Derek M.; Rovis, Tomislav
[Journal of the American Chemical Society, 2015, vol. 137, # 13, p. 4445 - 4452]
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