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CAS 252670-79-4 | (1-methoxynaphthalen-2-yl)boronic Acid

Molecular Formula: C11H11BO3
Molecular Weight: 202.01
Purity: 97% Min.
Package: 1 g / 5 g / 25 g / 100 g / 1 kg / 25 kg
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Specification of CAS 252670-79-4 | (1-methoxynaphthalen-2-yl)boronic acid

Synthesis of CAS 252670-79-4 | (1-methoxynaphthalen-2-yl)boronic acid

Conditions

Stage #1: 2-bromo-1-methoxynaphthalene With n-butyllithium In diethyl ether; hexane at -78℃; for 0.5h; Inert atmosphere;

Stage #2: Trimethyl borate In diethyl ether; hexane at -78 - 20℃; for 12h; Inert atmosphere;

Stage #3: With hydrogenchloride In water for 0.5h;

Reference

Bentley, Keith W.; Nam, Yea G.; Murphy, Jaslynn M.; Wolf, Christian

[Journal of the American Chemical Society, 2013, vol. 135, # 48, p. 18052 - 18055]

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