CAS 68817-71-0 | 2-AMINO-4'-CHLORODIPHENYLAMINE
Molecular Formula: C12H11ClN2
Molecular Weight: 218.68
EINECS: 272-391-8
Purity: 97% Min.
Package: 1 g / 5 g / 25 g / 100 g / 1 kg
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Product Introduction
Specification of CAS 68817-71-0 | 2-AMINO-4'-CHLORODIPHENYLAMINE
ITEMS | SPECIFICATION |
Melting point | 117-119 °C(lit.) |
InChIKey | WEUBIWJPIRTWDF-UHFFFAOYSA-N |
storage temp. | Keep in dark place,Inert atmosphere,Room temperature |
density | 1.288 g/cm3 |
Boiling point | 357.0 °C |
pka | 4.90 |
Synthesis of CAS 68817-71-0 | 2-AMINO-4'-CHLORODIPHENYLAMINE
Conditions
Stage #1: 3-fluorobromobenzene With magnesium In diethyl ether for 2h; Inert atmosphere; Reflux;
Stage #2: With phosphorus trichloride In diethyl ether for 1h; Reflux; Inert atmosphere;
Reference
Goto, Akihiro; Otake, Kazuki; Kubo, Ozora; Sawama, Yoshinari; Maegawa, Tomohiro; Fujioka, Hiromichi [Chemistry - A European Journal, 2012, vol. 18, # 36, p. 11423 - 11432]
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