CAS 709031-45-8 | Saxagliptin Intermediate
Molecular Formula: C7H14N2O4S
Molecular Weight: 222.26
EINECS: 615-206-1
Purity: 97% Min.
Package: 1 g / 5 g / 25 g / 100 g / 1 kg
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Product Introduction
Introduction
(1S,3S,5S)-2-Azabicyclo[3.1.0]hexane-3-carboxamide MonoMethanesulfonate is a saxagliptin intermediate.
Specification of CAS 709031-45-8 | 2-Azabicyclo[3.1.0]hexane-3-carboxaMide, (1S,3S,5S)-,MonoMethanesulfonate
ITEMS | SPECIFICATION |
storage temp. | Inert atmosphere,Room Temperature |
Synthesis of CAS 709031-45-8 | 2-Azabicyclo[3.1.0]hexane-3-carboxaMide, (1S,3S,5S)-,MonoMethanesulfonate
Conditions:
In isopropyl alcohol at 55 - 65℃; for 3.5h; Large scale reaction;
Reference:
Savage, Scott A.; Jones, Gregory S.; Kolotuchin, Sergei; Ramrattan, Shelly Ann; Vu, Truc; Waltermire, Robert E.
[Organic Process Research and Development, 2009, vol. 13, # 6, p. 1169 - 1176]
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