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CAS 473927-63-8 | Ethyl (2Z)-chloro[(4-methoxyphenyl)hydrazono]ethanoate
Molecular Formula: C11H13ClN2O3
Molecular Weight: 256.69
Purity: 97% Min.
Package: 1 g / 5 g / 25 g / 100 g / 1 kg / 25 kg
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Product Introduction
Specification of CAS 473927-63-8 | Ethyl (2Z)-chloro[(4-methoxyphenyl)hydrazono]ethanoate
ITEMS | SPECIFICATION |
Boiling point | 349.0 °C |
pka | 11.63 |
density | 1.23 |
Synthesis of CAS 473927-63-8 | Ethyl (2Z)-chloro[(4-methoxyphenyl)hydrazono]ethanoate
Conditions
Stage #1: 4-methoxy-aniline With hydrogenchloride; sodium nitrite at -5℃; for 0.5h; Stage #2: ethyl 2-chloro-3-oxo-butyrate With sodium acetate In water; acetone at 20℃; for 2h; Further stages.;
Reference
Pinto, Donald J. P.; Orwat, Michael J.; Koch, Stephanie; Rossi, Karen A.; Alexander, Richard S.; Smallwood, Angela; Wong, Paneras C.; (…) Wexler, Ruth R.; Lam, Patrick Y. S.
[Journal of Medicinal Chemistry, 2007, vol. 50, # 22, p. 5339 - 5356]
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