CAS 104206-65-7 | 2-(2-nitro-4-trifluoromethylbenzoyl)-1,3-cyclohexanedione
Molecular Formula: C14H10F3NO5
Molecular Weight: 329.23
EINECS: 691-056-0
Purity: 97% Min.
Package: 1 g / 5 g / 25 g / 100 g / 1 kg / 25 kg
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Product Introduction
Specification of CAS 104206-65-7 | 2-(2-nitro-4-trifluoromethylbenzoyl)-1,3-cyclohexanedione
ITEMS | SPECIFICATION |
Melting point | 129-131°C |
color | white to brown |
storage temp. | -20°C |
solubility | DMSO |
RTECS | GV0766666 |
form | Solid |
InChIKey | OUBCNLGXQFSTLU-UHFFFAOYSA-N |
density | 1.484 g/cm3 |
Boiling point | 486.2 °C |
pka | 3.13 |
EPA Substance Registry System | 1,3-Cyclohexanedione, 2-[2-nitro-4-(trifluoromethyl)benzoyl]- (104206-65-7) |
Synthesis of CAS 104206-65-7 | 2-(2-nitro-4-trifluoromethylbenzoyl)-1,3-cyclohexanedione
Conditions
Stage #1: 1,3-cylohexanedione With triethylamine In dichloromethane at 20℃; for 4h;
Stage #2: 2-nitro-4-trifluoromethyl-benzoyl chloride In dichloromethane at 0 - 20℃; for 1.25h;
Stage #3: With triethylamine; 2-hydroxy-2-methylpropanenitrile In dichloromethane at 40℃; for 1h;
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