CAS 2230887-26-8 | 4,4',4''-(pyridine-2,4,6-triyl)tribenzaldehyde
Molecular Formula: C26H17NO3
Molecular Weight: 391.43
Purity: 97% Min.
Package: 1 g / 5 g / 25 g / 100 g / 1 kg
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Product Introduction
Specification of CAS 2230887-26-8 | 4,4',4''-(pyridine-2,4,6-triyl)tribenzaldehyde
ITEMS | SPECIFICATION |
Boiling point | 602.0 °C |
pka | 2.08 |
Density | 1.248 g/cm3 |
Synthesis of CAS 2230887-26-8 | 4,4',4''-(pyridine-2,4,6-triyl)tribenzaldehyde
Conditions
Stage #1: 2,4,6 tris(4-bromophenyl)pyridine With n-butyllithium In tetrahydrofuran; hexane at -78 - -70℃; for 3h; Inert atmosphere;
Stage #2: N-Formylpiperidine In tetrahydrofuran; hexane at -78 - 20℃; for 17h; Inert atmosphere;
Reference
El-Mahdy, Ahmed F. M.; Kuo, Cheng-Han; Alshehri, Abdulmohsen; Young, Christine; Yamauchi, Yusuke; Kim, Jeonghun; Kuo, Shiao-Wei
[Journal of Materials Chemistry A, 2018, vol. 6, # 40, p. 19532 - 19541]
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