CAS 156682-53-0 | 3-Bromo-2-fluoro-phenol
Molecular Formula: C6H4BrFO
Molecular Weight: 191
Purity: 97% Min.
Package: 1 g / 5 g / 25 g / 100 g / 1 kg / 25 kg
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Product Introduction
Specification of CAS 156682-53-0 | 3-Bromo-2-fluoro-phenol
ITEMS | SPECIFICATION |
Boiling point | 207.4 °C |
pka | 7.74 |
Storage temp. | Sealed in dry,Room Temperature |
Density | 1.764 g/cm3 |
Synthesis of CAS 156682-53-0 | 3-Bromo-2-fluoro-phenol
Conditions
Stage #1: 1-bromo-2,3-difluorobenzene With potassium trimethylsilonate In diethylene glycol dimethyl ether at 120℃; for 5h; Inert atmosphere;
Stage #2: With hydrogenchloride In diethylene glycol dimethyl ether; water at 20℃; Inert atmosphere;
Reference
Li, Jianqing; Smith, Daniel; Qiao, Jennifer X.; Huang, Stella; Krishnananthan, Subramaniam; Wong, Henry S.; Salvati, Mark E.; Balasubramanian, Balu N.; Chen, Bang-Chi
[Synlett, 2009, # 4, p. 633 - 637]
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