CAS 1071125-59-1 | 4,4',4''-(benzene-1,3,5-triyltris(oxy))tribenzoic Acid
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CAS 1071125-59-1 | 4,4',4''-(benzene-1,3,5-triyltris(oxy))tribenzoic Acid

CAS 1071125-59-1 | 4,4',4''-(benzene-1,3,5-triyltris(oxy))tribenzoic Acid

Molecular Formula: C27H18O9
Molecular Weight: 486.43
Purity: 97% Min.
Package: 1 g / 5 g / 25 g / 100 g / 1 kg

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Product Introduction

Specification of CAS 1071125-59-1 | 4,4',4''-(benzene-1,3,5-triyltris(oxy))tribenzoic acid

ITEMS

SPECIFICATION

pka

3.72

Melting point

343.2 °C

Density

1.435 g/cm3

Boiling point

709.9 °C

Synthesis of CAS 1071125-59-1 | 4,4',4''-(benzene-1,3,5-triyltris(oxy))tribenzoic acid

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Conditions

Stage #1: 3,5-dihydroxyphenol; 4-fluorobenzonitrile With potassium carbonate In 1-methyl-pyrrolidin-2-one; toluene at 150℃; for 3h; Dean-Stark; Inert atmosphere;

Stage #2: In 1-methyl-pyrrolidin-2-one at 180℃; for 16h; Dean-Stark; Inert atmosphere;

Stage #3: With water; potassium hydroxide In ethanol at 80℃; for 12h;

Reference

Park, Hye Jeong; Oh, Jongbum; Kim, Jiwon; Kim, Jaheon

[Chemical Communications, 2020, vol. 56, # 67, p. 9727 - 9730]

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