CAS 199287-52-0 | Benzaldehyde, 4,5-difluoro-2-hydroxy- (9CI)

CAS 199287-52-0 | Benzaldehyde, 4,5-difluoro-2-hydroxy- (9CI)

Molecular Formula: C7H4F2O2
Molecular Weight: 158.1
EINECS: 642-799-4
Purity: 97% Min.
Package: 1 g / 5 g / 25 g / 100 g / 1 kg / 25 kg
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Product Introduction

Specification of CAS 199287-52-0 | Benzaldehyde, 4,5-difluoro-2-hydroxy- (9CI)

ITEMS

SPECIFICATION

Melting point

68-72℃

Storage temp.

Inert atmosphere,2-8°C

Density

1.464 g/cm3

Boiling point

224.1 °C

pka

7.20

Sensitive

Air Sensitive

Synthesis of CAS 199287-52-0 | Benzaldehyde, 4,5-difluoro-2-hydroxy- (9CI)

image

Conditions

Stage #1: 2-bromo-4,5-difluorophenol With n-butyllithium In tetrahydrofuran; hexanes at -78℃; for 0.5h;

Stage #2: N,N-dimethyl-formamide In tetrahydrofuran; hexanes at 20℃; for 18h;

Stage #3: With water In tetrahydrofuran; hexanes


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