
CAS 199287-52-0 | Benzaldehyde, 4,5-difluoro-2-hydroxy- (9CI)
Molecular Formula: C7H4F2O2
Molecular Weight: 158.1
EINECS: 642-799-4
Purity: 97% Min.
Package: 1 g / 5 g / 25 g / 100 g / 1 kg / 25 kg
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Product Introduction
Specification of CAS 199287-52-0 | Benzaldehyde, 4,5-difluoro-2-hydroxy- (9CI)
ITEMS | SPECIFICATION |
Melting point | 68-72℃ |
Storage temp. | Inert atmosphere,2-8°C |
Density | 1.464 g/cm3 |
Boiling point | 224.1 °C |
pka | 7.20 |
Sensitive | Air Sensitive |
Synthesis of CAS 199287-52-0 | Benzaldehyde, 4,5-difluoro-2-hydroxy- (9CI)

Conditions
Stage #1: 2-bromo-4,5-difluorophenol With n-butyllithium In tetrahydrofuran; hexanes at -78℃; for 0.5h;
Stage #2: N,N-dimethyl-formamide In tetrahydrofuran; hexanes at 20℃; for 18h;
Stage #3: With water In tetrahydrofuran; hexanes
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