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CAS 74472-22-3 | Allyl(tert-butyl)dimethylsilane
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CAS 74472-22-3 | Allyl(tert-butyl)dimethylsilane

CAS 74472-22-3 | Allyl(tert-butyl)dimethylsilane

Molecular Formula: C9H20Si
Molecular Weight: 156.34
Purity: 97% Min.
Package: 1 g / 5 g / 25 g / 100 g / 1 kg / 25 kg
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Product Introduction

Specification of CAS 74472-22-3 | Allyl(tert-butyl)dimethylsilane

ITEMS

SPECIFICATION

Boiling point

152°C(lit.)

Refractive index

1.4360-1.4400

Storage temp.

Inert atmosphere,2-8°C

Density

0.751 g/cm3

Synthesis of CAS 74472-22-3 | Allyl(tert-butyl)dimethylsilane

image

Conditions

Stage #1: allylmagnesium bromide; tert-butyldimethylsilyl chloride With N,N,N,N,-tetramethylethylenediamine In tetrahydrofuran at 20℃; for 8h; Inert atmosphere;

Stage #2: With water; ammonium chloride In tetrahydrofuran Inert atmosphere;

Reference

Murakami, Kei; Yorimitsu, Hideki; Oshima, Koichiro

[Journal of Organic Chemistry, 2009, vol. 74, # 3, p. 1415 - 1417]

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