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CAS 31865-25-5 | 6-Oxa-3-azabicyclo[3.1.0]hexane-3-carboxylic Acid, Phenylmethyl Ester
Molecular Formula: C12H13NO3
Molecular Weight: 219.24
Purity: 97% Min.
Package: 100 g / 1 kg / 25 kg
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Product Introduction
Specification of CAS 31865-25-5 | 6-Oxa-3-azabicyclo[3.1.0]hexane-3-carboxylic acid, phenylMethyl ester
ITEMS | SPECIFICATION |
Boiling point | 353.9 °C |
pka | -1.03 |
Storage temp. | 2-8°C |
Density | 1.305 g/cm3 |
Synthesis of CAS 31865-25-5 | 6-Oxa-3-azabicyclo[3.1.0]hexane-3-carboxylic acid, phenylMethyl ester
Conditions
Stage #1: 1-carboxybenzyl-3-pyrrolidine With 1,1,1-trifluoro-2-propanone; (ethylenedinitrilo)tetraacetic acid disodium salt In lithium hydroxide monohydrate; acetonitrile at 0℃; for 0.166667h;
Stage #2: With Potassium peroxomonosulfate; Sodium hydrogenocarbonate In lithium hydroxide monohydrate; acetonitrile at 0℃; for 2.16667h; pH=7;
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