CAS 25859-52-3 | Methyl 3-methyl-3-butenoate
Molecular Formula: C6H10O2
Molecular Weight: 114.14
Purity: 97% Min.
Package: 100 g / 1 kg / 25 kg
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Product Introduction
Synthesis of CAS 25859-52-3 | Methyl 3-methyl-3-butenoate
Conditions
Stage #1: malonic acid dimethyl ester With lithium hexamethyldisilazane In tetrahydrofuran at 0℃; for 1h; Inert atmosphere; Sealed tube;
Stage #2: 2-methyl-3-bromo-1-propene In tetrahydrofuran at 0 - 20℃; for 18h; Inert atmosphere; Sealed tube;
Reference
Di Bussolo, Valeria; Princiotto, Salvatore; Martinelli, Elisa; Bordoni, Vittorio; Crotti, Paolo [Tetrahedron Letters, 2016, vol. 57, # 15, p. 1644 - 1647]
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