CAS 877399-73-0 | 1-Piperidinecarboxylic Acid, 4-(4-iodo-1H-pyrazol-1-yl)-, 1,1-dimethylethyl Ester
Molecular Formula: C13H20IN3O2
Molecular Weight: 377.22
Purity: 97% Min.
Package: 1 g / 5 g / 25 g / 100 g / 1 kg / 25 kg
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Product Introduction
Specification of CAS 877399-73-0 | 1-Piperidinecarboxylic acid, 4-(4-iodo-1H-pyrazol-1-yl)-, 1,1-dimethylethyl ester
ITEMS | SPECIFICATION |
Melting point | 97 °C |
Storage temp. | Keep in dark place,Sealed in dry,2-8°C |
Form | Solid |
Density | 1.60 g/cm3 |
Boiling point | 430.6 °C |
pka | 1.08 |
Sensitive | Light Sensitive |
CAS DataBase Reference | 877399-73-0 |
Synthesis of CAS 877399-73-0 | 1-Piperidinecarboxylic acid, 4-(4-iodo-1H-pyrazol-1-yl)-, 1,1-dimethylethyl ester
Conditions
Stage #1: 4-iodopyrazole With sodium hydride In dichloromethane; mineral oil at 0℃; for 1h;
Stage #2: 1-(tert-butoxycarbonyl)piperidin-4-yl methanesulfonate In dichloromethane; mineral oil at 100℃; for 15h;
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