CAS 50650-59-4 | 2-Hydroxy-4-(trifluoromethyl)pyridine
Molecular Formula: C6H4F3NO
Molecular Weight: 163.1
EINECS: 610-554-0
Purity: 97% Min.
Package: 1 g / 5 g / 25 g / 100 g / 1 kg
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Product Introduction
Introduction
2-Hydroxy-4-(trifluoromethyl)pyridine is a fuorine-containing pyridine intermediate.
Specification of CAS 50650-59-4 | 2-Hydroxy-4-(trifluoromethyl)pyridine
ITEMS | SPECIFICATION |
Melting point | 161-165 °C (lit.) |
storage temp. | Inert atmosphere,Room Temperature |
solubility | Soluble in methanol. |
density | 1.398 g/cm3 |
Boiling point | 221.2 °C |
pka | 10.76 |
CAS DataBase Reference | 50650-59-4(CAS DataBase Reference) |
Synthesis of CAS 50650-59-4 | 2-Hydroxy-4-(trifluoromethyl)pyridine
Conditions:
With nickel(II) sulfate hexahydrate; 4,4'-Dimethoxy-2,2'-bipyridin; 8,9-bis((R)-2-acetoxypropyl)-7,10-dimethoxyperyleno[1,12-def][1,3]dioxepine-5,6,11,12-tetrayl tetraacetate; 18O-labeled water; N-ethyl-N,N-diisopropylamine In N,N-dimethyl-formamide; acetonitrile at 20℃; for 48h; Schlenk technique; Irradiation; Inert atmosphere;
Reference:
Guo, Baodang; Huang, Shuping; Li, Jia; Li, Min; Liu, Xuanzhong; Rao, Yijian; Wu, Yawen; Yin, Huimin; Yuan, Zhenbo; Zhang, Yan
[Journal of Catalysis, 2021, vol. 399, p. 111 - 120]
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