CAS 35034-22-1 | 2-Methyl-1H-imidazole-4-carbaldehyde

Specification of CAS 35034-22-1 | 2-Methyl-1H-imidazole-4-carbaldehyde

Synthesis of CAS 35034-22-1 | 2-Methyl-1H-imidazole-4-carbaldehyde

Conditions

Stage #1: N,N-dimethyl-2-methyl-1H-imidazole-1-sulfonamide With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 0.5h;

Stage #2: N,N-dimethyl-formamide In tetrahydrofuran; hexane at -78 - 20℃; Further stages.;

Reference

Madsen, Christian; Jensen, Anders A.; Liljefors, Tommy; Kristiansen, Uffe; Nielsen, Birgitte; Hansen, Camilla P.; Larsen, Mogens; (…) Krogsgaard-Larsen, Povl; Frølund, Bente

[Journal of Medicinal Chemistry, 2007, vol. 50, # 17, p. 4147 - 4161]

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