CAS 13670-99-0 | 1-(2,6-Difluorophenyl)ethan-1-one
Molecular Formula: C8H6F2O
Molecular Weight: 156.13
EINECS: 237-151-9
Purity: 97% Min.
Package: 1 g / 5 g / 25 g / 100 g / 1 kg / 25 kg
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Product Introduction
Specification of CAS 13670-99-0 | 1-(2,6-Difluorophenyl)ethan-1-one
ITEMS | SPECIFICATION |
color | Clear colorless to slightly yellow |
Fp | 170 °F |
Refractive index | n20/D 1.48(lit.) |
Form | Liquid |
Density | 1.197 g/mL at 25 °C(lit.) |
Boiling point | 76-79 °C15 mm Hg(lit.) |
Specific Gravity | 1.197 |
Water Solubility | Slightly soluble in water. |
NIST Chemistry Reference | Ethanone, 1-(2,6-difluorophenyl)-(13670-99-0) |
BRN | 2046068 |
CAS DataBase Reference | 13670-99-0(CAS DataBase Reference) |
Synthesis of CAS 13670-99-0 | 1-(2,6-Difluorophenyl)ethan-1-one
Conditions
Stage #1: 2,6 difluorobenzonitrile; methylmagnesium chloride In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene at 20℃; for 20h; Inert atmosphere;
Stage #2: With sulfuric acid In tetrahydrofuran; 5,5-dimethyl-1,3-cyclohexadiene; water at 50℃;
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