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CAS 116258-17-4 | (1S,4S)-(+)-2-Benzyl-2,5-diazabicyclo[2.2.1]heptane Dihydrobromide
Molecular Formula: C12H18Br2N2
Molecular Weight: 350.09
Purity: 97% Min.
Package: 1 g / 5 g / 25 g / 100 g / 1 kg
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Product Introduction
Specification of CAS 116258-17-4 | (1S,4S)-(+)-2-Benzyl-2,5-diazabicyclo[2.2.1]heptane dihydrobromide
ITEMS | SPECIFICATION |
Melting point | 270 °C (dec.)(lit.) |
alpha | 16.5 º (C=3 IN 2 M NAOH) |
refractive index | 16 ° (C=3, 2mol/L NaOH) |
optical activity | [α]20/D +16.5°, c = 3 in 2 M NaOH |
Water Solubility | very faint turbidity |
CAS DataBase Reference | 116258-17-4(CAS DataBase Reference) |
Synthesis of CAS 116258-17-4 | (1S,4S)-(+)-2-Benzyl-2,5-diazabicyclo[2.2.1]heptane dihydrobromide
Conditions
With hydrogen bromide at 110℃; for 0.5h; microwave irradiation;
Reference
Melgar-Fernandez, Roberto; Gonzalez-Olvera, Rodrigo; Olivares-Romero, J. Luis; Gonzalez-Lopez, Vianney; Romero-Ponce, Leticia; Ramirez-Zarate, Maria Del Refugio; Demare, Patricia; Regla, Ignacio; Juaristi, Eusebio
[European Journal of Organic Chemistry, 2008, # 4, p. 655 - 672]
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