296-35-5 | 1,4,7,10,13,16-Hexaazacyclooctadecane
Molecular Formula: C12H30N6
Molecular Weight: 258.41
EINECS: 206-042-8
Purity: 97% Min.
Package: 100 mg / 250 mg / 1 g
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Product Introduction
Introduction
1,4,7,10,13,16-Hexaazacyclooctadecane is a crown ether.
Specification of CAS: 296-35-5 1,4,7,10,13,16-HEXAAZACYCLOOCTADECANE
ITEMS | SPECIFICATION |
Melting point | 147-152 °C |
Storage temp. | Inert atmosphere,2-8°C |
BRN | 1105038 |
Synthesis of CAS: 296-35-5 1,4,7,10,13,16-HEXAAZACYCLOOCTADECANE
Multi-step reaction with 3 steps
1: 72 percent / 30percent NaOH / triethylbenzylammonium chloride / H2O; CH2Cl2 / 10 - 15 °C
2: 85 percent / 5percent NaOH / tetrabutylammonium iodide / H2O; toluene / Heating; 8-10 h
3: 75 percent / conc. H2SO4 / 100 - 105 °C / Heating; 50-70 h
Reference:
Luk'yanenko, N. G.; Basok, S. S.; Filonova, L. K.; Kulikov, N. V.; Pastushok, V. N.
[Chemistry of Heterocyclic Compounds, 1990, vol. 26, # 3, p. 346 - 349][Khimiya Geterotsiklicheskikh Soedinenii, 1990, # 3, p. 401 - 404]
Hot Tags: 296-35-5 | 1,4,7,10,13,16-hexaazacyclooctadecane, price, quotation, discount, in stock, for sale, Metal Catalysts, Catalyst Ligands
