CAS 408492-27-3 | 2,6-DICHLORO-4-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)PYRIDINE
Molecular Formula: C11H14BCl2NO2
Molecular Weight: 273.95
Purity: 97% Min.
Package: 1 g / 5 g / 25 g / 100 g / 1 kg
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Product Introduction
Specification of CAS 408492-27-3 | 2,6-DICHLORO-4-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)PYRIDINE
ITEMS | SPECIFICATION |
Melting point | 117-119°C |
InChIKey | PEFDHAOFDBNZEQ-UHFFFAOYSA-N |
Storage temp. | 2-8°C |
Density | 1.24 g/cm3 |
Boiling point | 373.2 °C |
pka | -3.74 |
CAS DataBase Reference | 408492-27-3 |
Synthesis of CAS 408492-27-3 | 2,6-DICHLORO-4-(4,4,5,5-TETRAMETHYL-1,3,2-DIOXABOROLAN-2-YL)PYRIDINE

Conditions
Stage #1: bis(pinacol)diborane With (1,5-cyclooctadiene)(methoxy)iridium(I) dimer; 4,4'-di-tert-butyl-2,2'-bipyridine In tert-butyl methyl ether Inert atmosphere;
Stage #2: 2,6-dichloropyridine In tert-butyl methyl ether at 80℃; for 0.05h; Inert atmosphere; Microwave irradiation;
Reference
Harrisson, Peter; Morris, James; Marder, Todd B.; Steel, Patrick G.
[Organic Letters, 2009, vol. 11, # 16, p. 3586 - 3589]
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