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CAS 2117-12-6 | 4-TRIMETHYLSILYL-3-BUTYN-1-OL

Molecular Formula: C7H14OSi
Molecular Weight: 142.27
Purity: 97% Min.
Package: 1 g / 5 g / 25 g / 100 g / 1 kg / 25 kg
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Specification of CAS 2117-12-6 | 4-TRIMETHYLSILYL-3-BUTYN-1-OL

ITEMS	SPECIFICATION
Color	Clear to opaque grey to brown-black
Fp	50.1 ℃
Refractive index	1.4536
Form	Solution
Density	0.854
Boiling point	97 °C
Specific Gravity	0.854
pka	14.61
CAS DataBase Reference	2117-12-6

Synthesis of CAS 2117-12-6 | 4-TRIMETHYLSILYL-3-BUTYN-1-OL

Conditions

Stage #1: 3-Butyn-1-ol With n-butyllithium In tetrahydrofuran; hexane at -78 - 20℃; for 1h;

Stage #2: chloro-trimethyl-silane In tetrahydrofuran; hexane at -78 - 20℃; for 2h

Reference

Harms, Vanessa; Schröder, Benjamin; Oberhauser, Clara; Tran, Cong Duc; Winkler, Sven; Dräger, Gerald; Kirschning, Andreas

[Organic Letters, 2020, vol. 22, # 11, p. 4360 - 4365]

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