CAS 1345866-66-1 | 4-(6-methyl-1,2,4,5-tetrazin-3-yl)-Benzoic Acid
Molecular Formula: C10H8N4O2
Molecular Weight: 216.2
Purity: 97% Min.
Package: 25 mg / 100 mg / 1 g / 5 g
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Product Introduction
Specification of CAS 1345866-66-1 | Benzoic acid, 4-(6-methyl-1,2,4,5-tetrazin-3-yl)-
ITEMS | SPECIFICATION |
Boiling point | 483.2 °C |
pka | 3.06 |
Density | 1.382 g/cm3 |
Synthesis of CAS 1345866-66-1 | Benzoic acid, 4-(6-methyl-1,2,4,5-tetrazin-3-yl)-
Conditions
Stage #1: 4-cyanobenzoic Acid; acetonitrile With zinc trifluoromethanesulfonate; hydrazine hydrate at 60℃; for 13h; Inert atmosphere;
Stage #2: With hydrogenchloride; sodium nitrite In water at 20℃; pH=3;
Reference
Linden, Greta; Zhang, Lei; Pieck, Fabian; Linne, Uwe; Kosenkov, Dmitri; Tonner, Ralf; Vázquez, Olalla [Angewandte Chemie - International Edition, 2019, vol. 58, # 37, p. 12868 - 12873]
[Angew. Chem., 2019, vol. 131, p. 13000 - 13005,6]
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