CAS 1028648-22-7 | 9-(biphenyl-4-yl)-3-boricacid-9H-carbazole
Molecular Formula: C24H18BNO2
Molecular Weight: 363.22
Purity: 97% Min.
Package: 1 g / 5 g / 25 g / 100 g / 1 kg / 25 kg
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Product Introduction
Specification of CAS 1028648-22-7 | 9-(biphenyl-4-yl)-3-boric acid-9H-carbazole
ITEMS | SPECIFICATION |
Boiling point | 555.9 °C |
pka | 8.81 |
density | 1.18 g/cm3 |
Synthesis of CAS 1028648-22-7 | 9-(biphenyl-4-yl)-3-boric acid-9H-carbazole
Conditions
Stage #1: 9-[1,1′-biphenyl-4-yl]-3-bromo-9H-carbazole With n-butyllithium In tetrahydrofuran; hexane at -78℃; for 2h;
Stage #2: Trimethyl borate In tetrahydrofuran; hexane at -78 - 20℃; for 20h; Stage #3: With hydrogenchloride; water In tetrahydrofuran; hexane at 20℃; for 3h;
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