CAS 81998-04-1 | 4-HydroxyMethyl-4'-Methyl-2,2'-bipyridyl
Molecular Formula: C12H12N2O
Molecular Weight: 200.24
Purity: 97% Min.
Package: 1 g / 5 g / 25 g / 100 g / 1 kg
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Product Introduction
Introduction
4-HydroxyMethyl-4'-Methyl-2,2'-bipyridyl is a pyridine derivative and can be used as an intermediate for synthetic materials.
Specification of CAS 81998-04-1 | 4-HydroxyMethyl-4'-Methyl-2,2'-bipyridyl
ITEMS | SPECIFICATION |
Melting point | 119.0 to 123.0 °C |
CAS DataBase Reference | 81998-04-1 |
Storage temp. | Inert atmosphere,Room Temperature |
Synthesis of CAS 81998-04-1 | 4-HydroxyMethyl-4'-Methyl-2,2'-bipyridyl
Conditions
Stage #1: 4,4'-dimethyl-2,2'-bipyridines With selenium(IV) oxide In 1,4-dioxane at 105℃; for 48h; Inert atmosphere;
Stage #2: With sodium tetrahydroborate; sodium hydroxide In methanol at 0 - 20℃; for 2.5h; Inert atmosphere;
Reference
Zhou; Chen; Bai; Sun; Li; Qiao
[Organic and Biomolecular Chemistry, 2017, vol. 15, # 32, p. 6738 - 6745]
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