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CAS 13315-17-8 | BIS (P-DIMETHYLSILYL) PHENYL ETHER

Molecular Formula: C16H22OSi2
Molecular Weight: 286.52
Purity: 97% Min.
Package: 1 g / 5 g / 25 g / 100 g / 1 kg / 25 kg
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Specification of CAS 13315-17-8 | BIS (P-DIMETHYLSILYL) PHENYL ETHER

ITEMS	SPECIFICATION
Melting point	<25°C
storage temp.	Inert atmosphere,Room Temperature
Fp	>110°C
refractive index	1.5478
density	0.976
Boiling point	138 °C
Specific Gravity	0.976
Hydrolytic Sensitivity	3

Synthesis of CAS 13315-17-8 | BIS (P-DIMETHYLSILYL) PHENYL ETHER

Conditions

Stage #1: 4-dimethylsilylphenylmagnesium bromide With 1,2,3-Benzotriazole; copper(l) iodide In dimethyl sulfoxide at 20℃; for 0.5h;

Stage #2: 4-(dimethylsilyl)phenol With sodium t-butanolate In dimethyl sulfoxide at 95 - 100℃; for 18h;

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