CAS 184950-35-4 | (TETRAHYDROFURAN-3-YL)METHANAMINE HYDROCHLORIDE
Molecular Formula: C5H12ClNO
Molecular Weight: 137.61
EINECS: 687-291-3
Purity: 97% Min.
Package: 1 g / 5 g / 25 g / 100 g / 1 kg
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Product Introduction
Specification of CAS 184950-35-4 | (TETRAHYDROFURAN-3-YL)METHANAMINE HYDROCHLORIDE
ITEMS | SPECIFICATION |
Melting point | 72-92 °C |
Storage temp. | Keep in dark place,Inert atmosphere,2-8°C |
Synthesis of CAS 184950-35-4 | (TETRAHYDROFURAN-3-YL)METHANAMINE HYDROCHLORIDE
Conditions
Stage #1: tetrahydrofuran-3-carboxaldehyde With hydrogen; ammonium chloride; Raney nickel In methanol; water at 20℃; under 2068.65 Torr; for 16h;
Stage #2: di-tert-butyl dicarbonate With sodium hydroxide In 1,4-dioxane; water at 20℃; for 16h;
Stage #3: With hydrogenchloride In 1,4-dioxane
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