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CAS 6999-03-7 | 1-BROMO-4-TRIMETHYLSILYLBENZENE
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CAS 6999-03-7 | 1-BROMO-4-TRIMETHYLSILYLBENZENE

CAS 6999-03-7 | 1-BROMO-4-TRIMETHYLSILYLBENZENE

Molecular Formula: C9H13BrSi
Molecular Weight: 229.19
Purity: 97% Min.
Package: 1 g / 5 g / 25 g / 100 g / 1 kg / 25 kg
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Product Introduction

Specification of CAS 6999-03-7 | 1-BROMO-4-TRIMETHYLSILYLBENZENE

ITEMS

SPECIFICATION

Melting point

95-96 °C

InChIKey

UKTSSJJZFVGTCG-UHFFFAOYSA-N

storage temp.

Sealed in dry,Room Temperature

Fp

205 °F

Refractive index

n20/D 1.529(lit.)

Density

1.173 g/mL at 25 °C(lit.)

Boiling point

229.5 °C752 mm Hg(lit.)

Synthesis of CAS 6999-03-7 | 1-BROMO-4-TRIMETHYLSILYLBENZENE

image

Conditions

Stage #1: 1.4-dibromobenzene With n-butyllithium In diethyl ether; hexane at -78℃; for 4h;

Stage #2: chloro-trimethyl-silane In diethyl ether; hexane at -78 - 20℃; for 2.16667h;

Reference

Itami, Kenichiro; Terakawa, Koji; Yoshida, Jun-ichi; Kajimoto, Okitsugu

[Journal of the American Chemical Society, 2003, vol. 125, # 20, p. 6058 - 6059]

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